Can Label | Sample Volume (cm3) | Inner Dimensions (mm(in)) | Drawing (PDF) | Picture |
---|---|---|---|---|
A | 1.6 | 6.35(0.25)Ø x 63.5(2.5) | NIST 14-0542 | |
B | 3.9 | 9.53(0.375)Ø x 63.5(2.5) | NIST 14-0574 | |
C | 5.3 | 11.1(0.438)Ø x 63.5(2.5) | NIST 14-0577 | |
D | 6.9 | 12.7(0.50)Ø x 63.5(2.5) | NIST 14-0575 | |
E | 10.8 | 15.9(0.625)Ø x 63.5(2.5) | NIST 14-0540 |
Sample Envrionment Equipment Compatability List
- Powder Diffractometer Room Temperature Sample Changer
- Powder Diffractometer Low Temperature Pulse Tube
- Closed Cycle Refrigerators - low & high temperature
- Top Loading CCR - Long and Short, DCS & HFBS
- Orange Cryostat - 50 mm, 70 mm, & 100mm
- 3He Cryostat Big Blue
- SD-55
- 3He Cryostats
- BNL - Air/Vacuum Furnace
- 7 Tesla Superconducting Magnet with either the CT insert of 3He insert
Sample Holder Assembly
To assemble the vanadium powder sample holders require the sample holder, the lid and 6-32 screws, and indium, lead or viton o-ring to make a seal are needed. If you need to have a helium atmosphere for the experiment and the sample is not radioactive place all materials in glove box in the high bay and follow instructions on the box to use the helium gas (if the sample is radioactive contact a member of the user services team to help with inert atmosphere). Place the power in the sample holder. Put the correct length of indium or lead around the grove for the o-ring. If the sample will only be used at room temperature use a viton o-ring with the sample (this helps prevent powder from escaping the sample holder). Place the lid on the sample holder and screw in the 6-32 screws in a star pattern to properly compress the lead/indium o-ring.